Repozytorium

Quantification of active ingredients in Potentilla tormentilla by Raman and infrared spectroscopy.

Autorzy

Sylwester Mazurek

Izabela Fecka

Magdalena Węglińska

Roman Szostak

Rok wydania

2018

Czasopismo

Talanta

Numer woluminu

189

Strony

308-314

DOI

10.1016/j.talanta.2018.07.012

Kolekcja

Naukowa

Język

Angielski

Typ publikacji

Artykuł

Streszczenie

The most important active compounds present in Potentilla tormentilla rhizomes were quantitatively determined on the basis of Raman, attenuated total reflection (ATR) and diffuse reflectance mid- and near- infrared spectra (DRIFTS) collected for the untreated plant material. Partial least-squares (PLS) models were constructed utilizing vibrational spectra and the results of reference high-performance liquid chromatography analyses. Applying Raman spectroscopy, total polyphenols, tannins, ellagitannins, procyanidins, agrimoniin, 3-O-galloylquininc acid and catechin were simultaneously quantified in tormentil rhizomes, with the relative standard errors of prediction in the 2.0–4.9% range for both calibration and validation sets. These error ranges were found to be slightly higher for infrared techniques and amounted to 2.7–6.5%.

Słowa kluczowe

potentilla, polyphenols, tannins, vibrational spectroscopy, quantitative analysis, multivariate analysis

Adres publiczny

https://doi.org/10.1016/j.talanta.2018.07.012

Strona internetowa wydawcy

http://www.elsevier.com

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