Repozytorium

Structural, spectroscopic and magnetic properties of new copper(II) complexes with a terpyridine ligand.

Autorzy

Monika Wałęsa-Chorab

Artur R. Stefankiewicz

Adam Gorczyński

Maciej Kubicki

Julia Kłak

Maria J. Korabik

Violetta Patroniak

Rok wydania

2011

Czasopismo

Polyhedron

Numer woluminu

30

Strony

233-240

DOI

10.1016/j.poly.2010.10.024

Kolekcja

Naukowa

Język

Angielski

Typ publikacji

Artykuł

Streszczenie

Four mononuclear complexes of the dimethylterpyridine ligand 1,3-bis(6-methylpyridin-2-yl)pyridine, L, C17H15N3, of the general formula CuLX2 were prepared from different copper(II) salts (X = Cl-1a, Br-1b, -1c and -1d). Their properties have been characterized through analytical, spectroscopic (EPR, ESI-MS, and IR) and magnetic measurements. Single crystal X-ray structure analyses of these complexes revealed five-coordinate metal ions in 1a, 1b and 1c, whereas 1d turned out to contain a six-coordinate Cu(II) center and to have both unique magnetic and structural properties, rationalized in terms of the hydrogen-bonding interactions seen in its crystal lattice.

Słowa kluczowe

Coordination modes, copper, magnetic properties

Adres publiczny

https://doi.org/10.1016/j.poly.2010.10.024

Strona internetowa wydawcy

http://www.elsevier.com

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