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Single crystal X-ray structure of 2,6-di-tert-butyl-4-(3-(4-chlorophenyl)-4-methyl-4,5-dihydroisoxazol-5-yl)phenol 1,4-dioxane hemisolvate.
Autorzy
Rok wydania
2013
Czasopismo
Journal of Structural Chemistry
Numer woluminu
54
Strony
217-222
DOI
10.1134/S0022476613010368
Kolekcja
Język
Angielski
Typ publikacji
Artykuł
The title compound (2,6-di-tert-butyl-4-(3-(4-chlorophenyl)-4-methyl-4,5-dihydroisoxazol-5-yl)phenol is synthesized and studied by the single crystal X-ray diffraction method. The structure of the product was confirmed by IR, 1H and 13C NMR spectroscopy. The crystal structure of 1,4-dioxane hemisolvate of the product is solved in the monoclinic space group P21/c with a = 17.713(6) Å, b = 9.529(3) Å, c = 13.972(4) Å, β = 94.09(4)°, V = 2352.3(13) Å3, Z = 4, T = 120(2) K.
Słowa kluczowe
single crystal X-ray structure, quinone methid e, isoxazoline, oxime, DDQ.
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