Repozytorium

Molecular and crystal structures of N-methyl-N-nitro- 2-chloroaniline.

Autorzy

V. V. Prezhdo

A. S. Bykova

Tadeusz Głowiak

Z. Daszkiewicz

Aleksander Koll

J. B. Kyzioł

N. E. Zhukhlistova

Rok wydania

2001

Czasopismo

Crystallography Reports

Numer woluminu

46

Strony

389-393

DOI

10.1134/1.1376466

Kolekcja

Naukowa

Język

Angielski

Typ publikacji

Artykuł

Streszczenie

The crystal structure of N-methyl-N-nitro-2-chloroaniline is determined by X-ray diffraction [a = 9.218(2) Å, b = 12.593(3) Å, c = 14.510(2) Å, space group Pbca, and Z = 8]. The structure is solved by the direct method and refined in the anisotropic approximation to R = 0.0377. All hydrogen atoms are localized. The structural parameters obtained agree with the data of the ab initio quantum-chemical B3LYP/6-31G** calculations. The data obtained are compared with those for N-methyl-N-nitro-4-chloroaniline. Conclusions on the interaction of the functional groups in the molecule are drawn.

Adres publiczny

https://doi.org/10.1134/1.1376466

Strona internetowa wydawcy

http://link.springer.com

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