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Inne
Carbacylamidophosphates: synthesis, properties and structure of dimorfolido-N-trichloroacetylphosphorylamide.
Autorzy
Rok wydania
1998
Czasopismo
Zeitschrift für Naturforschung Section B: A Journal of Chemical Sciences
Numer woluminu
53b
Strony
481-484
DOI
10.1515/znb-1998-0415
Kolekcja
Język
Angielski
Typ publikacji
Artykuł
Dimorpholido-N-trichloroacetylphosphorylamide: CCl3C(O)NHP(O)[N(CH2CH2)2O]2 [HL] and its sodium [NaL] and morpholine [HN(CH2-CH2)2O•HL] salts were synthesized for the first time. The compounds were studied by IR spectroscopy and assignments of the characteristic IR bands have been made. The structure of [HL] was determined by X-ray diffraction. Crystals are monoclinic, a = 11.412(2) Å, b = 16.056(3) Å, c = 9.622(2) Å, β = 108.55(3)°, space group P21/c; Z = 4. The refinement of the structure converged at R = 0.066. The molecules are connected into centrosymmetric dimers via hydrogen bonds formed by the phosphorylic oxygen atoms and hydrogen atoms of amide groups.
Słowa kluczowe
Carbacylamidophosphates, IR Data, X-Ray Dat
Adres publiczny
https://doi.org/10.1515/znb-1998-0415
Strona internetowa wydawcy
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