Repozytorium

Thermal quenching mechanisms of the Eu3+ luminescence in Ca9Al(PO4)7 obtained by citric route.

Autorzy

Robert Pązik

Katarzyna Zawisza

Adam Watras

Kinga Maleszka-Bagińska

Philippe Boutinaud

Rachid Mahiou

Przemysław J. Dereń

Rok wydania

2013

Czasopismo

Materials Research Bulletin

Numer woluminu

48

Strony

337-342

DOI

10.1016/j.materresbull.2012.10.034

Kolekcja

Naukowa

Język

Angielski

Typ publikacji

Artykuł

Streszczenie

The citric route was employed for synthesis of the pure phase Ca9Al(PO4)7:Eu3+ (CAlP:Eu3+) powders as an attractive alternative to the solid state reaction (no need of multistep and long thermal treatment). Structural properties of the final product were studied by means of X-ray diffraction as well as Rietveld refinement was conducted in order to calculate the cell parameters. The thermal behavior of the emission was studied using excitation line well matched with the 7F0 → 5D4 absorption band covering broad range of temperature. Activation energy was estimated to be equal to 10,550 cm−1. The thermal behavior of the Eu3+ luminescence in CAlP crystal lattice shown that the almost 80% of intensity is kept up to 430 K.

Słowa kluczowe

Inorganic compounds, optical materials, Chemical synthesis, luminescence

Adres publiczny

http://dx.doi.org/10.1016/j.materresbull.2012.10.034

Strona internetowa wydawcy

http://www.elsevier.com

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