Repozytorium
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Kolekcje
Inne
Vibrational, XRD and 13C NMR studies of DL-phenylglycinium methanesulfonate crystal.
Autorzy
Rok wydania
2016
Czasopismo
Spectrochimica Acta Part A-Molecular and Biomolecular Spectroscopy
Numer woluminu
168
Strony
139-147
DOI
10.1016/j.saa.2016.05.046
Kolekcja
Język
Angielski
Typ publikacji
Artykuł
A new crystal formed by DL-phenylglycine and methanesulfonic acid (PGLYMS) was obtained and studied by X-ray diffraction, IR and Raman spectroscopy, solid state NMR and DSC methods. Additionally, theoretical computations for the phenylglycine cation were carried out (DFT/B3LYP/aug-cc-pVDZ). Our results show that PGLYMS does not exhibit any phase transitions and crystallizes in the P21/c space group of monoclinic system (Z=4). Detailed analysis of its structure and its IR, Raman and NMR spectra is presented
Słowa kluczowe
hydrogen bonds, iR spectroscopy, Methanesulfonic anion, Phenylglycinium cation, Solid state NMR spectroscopy
Adres publiczny
http://dx.doi.org/10.1016/j.saa.2016.05.046
Strona internetowa wydawcy
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