Repozytorium

Synthesis, crystal structures and spectral characterization of chiral 4-R-1,2,4-triazoles.

Autorzy

Il’ya A. Gural’skiy

Viktor A. Reshetnikov

Irina V. Omelchenko

Agnieszka Szebesczyk

Elżbieta Gumienna-Kontecka

Igor O. Fritsky

Rok wydania

2017

Czasopismo

Journal of Molecular Structure

Numer woluminu

1127

Strony

164-168

DOI

10.1016/j.molstruc.2016.07.094

Kolekcja

Naukowa

Język

Angielski

Typ publikacji

Artykuł

Streszczenie

1,2,4-triazoles attract attention as actively used medications and ligands for constructing coordination architectures. In this paper we describe four optically active 4-substituted 1,2,4-triazoles that have been prepared by Bayer's synthesis from the corresponding aliphatic chiral amines. This approach tends to be universal towards different triazoles and permits to conserve a homochirality of substrates. Novel asymmetric molecules have been characterized by spectroscopic techniques and their structures have been retrieved from the single crystal X-ray analysis. Chiro-optical studies of these heterocycles have been made by means of circular dichroism spectroscopy.

Słowa kluczowe

Triazoles, Chirality, crystal structure, Circular dichroism, synthesis

Adres publiczny

http://dx.doi.org//10.1016/j.molstruc.2016.07.094

Strona internetowa wydawcy

http://www.elsevier.com

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