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Synthesis and X-ray single crystal structure analysis of a new 2-chlorobenzyl ammonium salt of phosphonic acid.
Autorzy
Rok wydania
2017
Czasopismo
Phosphorus, Sulfur, and Silicon and the Related Elements
Numer woluminu
192
Strony
638-642
DOI
10.1080/10426507.2017.1284837
Kolekcja
Język
Angielski
Typ publikacji
Artykuł
An efficient synthesis of a new 2-chlorobenzyl ammonium salt of phosphonic acid from the reaction of diethyl phosphite with 2-chlorobenzyl amine is described at moderate temperature in catalyst- and solvent-free conditions. The structure of this phosphonic acid salt was confirmed by FT-IR, 1H, 13C, and 31P NMR spectroscopy, and single crystal X-ray structure analysis.
Słowa kluczowe
2-Chlorobenzyl ammonium salt of phosphonic acid, catalyst-free, diethyl phosphite, single crystal X-ray structure, solvent-free
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