Repozytorium

Synthesis of thiazole aminophosphine oxides, aminophosphonic and aminophosphinic acids and Cu(II) binding abilities of thiazole aminophosphonic acids.

Autorzy

Tomasz K. Olszewski

Bogdan Boduszek

Sylwia Sobek

Henryk Kozłowski

Rok wydania

2006

Czasopismo

Tetrahedron

Numer woluminu

62

Strony

2183-2189

DOI

10.1016/j.tet.2005.12.016

Kolekcja

Naukowa

Język

Angielski

Typ publikacji

Artykuł

Streszczenie

A series of new aminophosphine oxides, aminophosphonic and aminophosphinic acids derived from thiazole was synthesized by addition of phosphine oxides or silylated phosphorus esters to the corresponding thiazole aldimines. The thiazole aldimines were obtained from 2-thiazole aldehyde and primary amines by a standard procedure. The corresponding phosphine oxides were obtained by alkylation of diethyl phosphite or ethyl phenylphosphinate with the appropriate Grignard reagents. The silylated phosphorus esters were prepared from trimethyl phosphite and from methyl- or phenylphosphinic ethyl ester by treatment with bromotrimethylsilane. The coordination ability towards Cu(II) ions are described for two obtained aminophosphonate ligands.

Adres publiczny

https://doi.org/10.1016/j.tet.2005.12.016

Strona internetowa wydawcy

http://www.elsevier.com

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