Repozytorium

Competition between the albumin and three histidine fragment of amyloid precursor protein sites to bind Cu(II).

Autorzy

Anna Janicka-Kłos

P. Juszczyk

Z. Grzonka

Henryk Kozłowski

Rok wydania

2008

Czasopismo

Polyhedron

Numer woluminu

27

Strony

1511-1516

DOI

10.1016/j.poly.2008.01.025

Kolekcja

Naukowa

Język

Angielski

Typ publikacji

Artykuł

Streszczenie

The aim of this work was to check experimentally the relationship between the five-nitrogen donor system {3 × Nimid, 2 × N} seen e.g. in the peptide fragments of the cysteine-rich amyloid precursor protein (APP) region and the albumin-like {NH2, 2 × N, Nimid} coordination site. The protected and unprotected octadecapeptides DAHQERMDVSETHLHWHT and Ac-DAHQERMDVSETHLHWHT-NH2 were synthesized and potentiometric and spectroscopic studies were performed. A comparison of both metal-binding sites that occur in both peptides clearly shows that in the unprotected ligand albumin-like binding is much more efficient than the three His site, although around pH 5 both sites have a comparable ability to bind the Cu(II) ion. However, a comparison of the protected and unprotected peptides with their metal binding sites clearly shows that the three His site is very efficient in binding Cu(II) although less effective than the albumin-like motif.

Adres publiczny

https://doi.org/10.1016/j.poly.2008.01.025

Strona internetowa wydawcy

http://www.elsevier.com