Repozytorium

Molecular dynamics and phase transitions in tris(dimethylammonium) enneaiododibismuthate(III) as studied by DSC, dilatometric, IR, 1H NMR and dielectric methods.

Autorzy

Ryszard Jakubas

Grażyna Bator

Lucjan Sobczyk

J. Zaleski

R. Decressain

J. Lefebvre

Rok wydania

1994

Czasopismo

Phase Transitions

Numer woluminu

46

Strony

257-267

DOI

10.1080/01411599408200331

Kolekcja

Naukowa

Język

Angielski

Typ publikacji

Artykuł

Streszczenie

The phase transitions and molecular motions of the cations were studied in the temperature range 130–300 K in a [(CH3)2NH2]3Bi2I9 (DMAIB) crystal by DSC, IR, dilatometric, dielectric and 1H NMR methods. It was confirmed that DMAIB undergoes three phase transitions at T c1 = 305 K, T c2 = 285 K and T c3 = 235 K. In the high-temperature phases I–II the cations undergo isotropic reorientations, and in phases III–IV both C3(CH3) motion and n-fold ionic reorientations take place.

Słowa kluczowe

Alkylammonium halogenobismuthates, phase transition, Infrared, dielectric, thermal expansion, NMR

Adres publiczny

https://doi.org/10.1080/01411599408200331

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