Repozytorium

Single crystal X-ray structure of 2-[({[(4-methylphenyl)sulfonyl]methyl}amino)carbonyl]-1,3-dioxo-2,3-dihydro-1H-iden-2-yl,2-thiophenecarboxylate.

Autorzy

Ali Ramazani

A. R. Kazemizadeh

Katarzyna Ślepokura

Tadeusz Lis

Rok wydania

2011

Czasopismo

Journal of Structural Chemistry

Numer woluminu

52

Strony

1085-1090

DOI

10.1134/S0022476611060072

Kolekcja

Naukowa

Język

Angielski

Typ publikacji

Artykuł

Streszczenie

The title compound 2-[({[(4-methylphenyl)sulfonyl]methyl}amino)carbonyl]-1,3-dioxo-2,3-dihydro-1H-inden-2-yl 2-thiophenecarboxylate is synthesized and studied by the single crystal X-ray diffraction method. The structure of the product is confirmed by IR, 1H and 13C NMR spectroscopy, and mass spectrometry. The structure is solved in the C2/c monoclinic space group with a = 16.739(3) Å, b = 11.087(3) Å, c = 23.194(4) Å, β = 93.32(3)°, V = 4297.2(16) Å3, Z = 8, R1 = 0.033 and wR2 = 0.088.

Adres publiczny

https://doi.org/10.1134/S0022476611060072

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