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Inne
Synthesis and crystal structure of methyl 2-(diphenylamino)-4-phenyl-1,3-thiazole-5-carboxylate.
Autorzy
Rok wydania
2013
Czasopismo
Chinese Journal of Structural Chemistry
Numer woluminu
32
Strony
82-88
Kolekcja
Język
Angielski
Typ publikacji
Artykuł
The title compound, methyl 2-(diphenylamino)-4-phenyl-1,3-thiazole-5- carboxylate, was synthesized and studied by single-crystal X-ray diffraction method. The structure of the product was confirmed by IR, 1H- and 13C-NMR spectroscopy and elemental analysis. These experimental studies were supported by quantum mechanical calculations. The structure was solved in monoclinic, space group P21/c with a = 9.573(3), b = 19.533(7), c = 9.876(3) Å, β = 92.35(4)°, V = 1845.2(10) Å3, T = 85(2) K, Z = 4, R = 0.040 and wR = 0.089 for 6424 observed reflections with I > 2s(I).
Słowa kluczowe
single-crystal X-ray structure, multi-component reaction, methyl 2-(diphenylamino)- 4-phenyl-1, 3-thiazole-5-carboxylate, benzoyl isothiocyanate, diphenylamine, dimethyl acetylenedicarboxylate
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