Repozytorium

Structural and spectroscopic properties of complexes formed between HNCS and SO2 in low temperature matrices.

Autorzy

Justyna Krupa

Maria Wierzejewska

Rok wydania

2017

Czasopismo

Spectrochimica Acta Part A-Molecular and Biomolecular Spectroscopy

Numer woluminu

183

Strony

144-149

DOI

10.1016/j.saa.2017.04.049

Kolekcja

Naukowa

Język

Angielski

Typ publikacji

Artykuł

Streszczenie

Matrix isolation FTIR spectroscopy has been combined with quantum chemical calculations in the aim to characterize complexes of isothiocyanic acid HNCS with SO2. The geometries of the 1:1, 1:2 and 2:1 complexes were optimized at the MP2 and DFT (B3LYPD3) levels of theory with the 6-311++G(3df,3pd) basis set. Five different HNCS ⋯ SO2 structures of the 1:1 stoichiometry were optimized. Three of them involve a weak Nsingle bondH ⋯ O hydrogen bond whereas two other geometries are stabilized by van der Waals interactions of various types. The HNCS/SO2/Ar spectra analysis evidences that at least one of the three hydrogen bonded structure is present after deposition of the matrices whereas the most stable van der Waals HNCS ⋯ SO2 structure as well as complexes of the 1:2 stoichiometry were detected upon annealing.

Słowa kluczowe

DFT/MP2, hydrogen bonds, van der Waals interaction, infrared spectra, matrix isolation

Adres publiczny

http://dx.doi.org/10.1016/j.saa.2017.04.049

Strona internetowa wydawcy

http://www.elsevier.com

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