Repozytorium
Wyszukaj
Kolekcje
Inne
Crystal structure of 2-[benzyl-(7-oxo-cyclohepta-1,3,5-trienyl)-amino]-Ncyclohexylpropanamide.
Autorzy
Rok wydania
2015
Czasopismo
Journal of Structural Chemistry
Numer woluminu
56
Strony
468-471
DOI
10.1134/S0022476615030105
Kolekcja
Język
Angielski
Typ publikacji
Artykuł
The title compound 2-[benzyl-(7-oxo-cyclohepta-1,3,5-trienyl)-amino]-N-cyclohexylpropanemide is synthesized and studied by the single crystal X-ray diffraction method. The structure of the product was confirmed by IR, 1H and 13C NMR spectroscopy, and mass spectrometry. The tropone oxygen atom plays an important role in the solid-state molecular structure stabilization by being involved in intramolecular N-H⋯O and C-H⋯O contacts.
Słowa kluczowe
single crystal X-ray structure, Smiles rearrangement, Ugi-type coupling, tropolone cyclohexylisocyanide, benzyl amine, acetaldehyde, Ugi-Smiles-type reaction
Adres publiczny
Podobne publikacje
Suzuki-Miyaura and Hiyama coupling catalyzed by PEPPSI-type complexes with non-bulky NHC ligand.
Osińska Marta, Gniewek Andrzej, Trzeciak Anna M.
Synthesis and single crystal X-ray structure of bis[4-oxo-3-(2-ethoxycarbonylphenyl)-3,4-dihydroquinazolin-2-yl]disulfide.
Rimaz M., Khalafy Jabbar, Tavana K., Ślepokura Katarzyna, Lis Tadeusz, Souldozi Ali, Mahyari Amir Tofangchi, Shajari N., Ramazani Ali
Single crystal X-ray structural analysis of two polymorphs of ethyl 2-(2-chlorophenyl)-4-hydroxy-5-oxo-1-phenyl-2,5-dihydro-1H-pyrrole-3-carboxylate.
Ramazani Ali, Ahankar Hamideh, Ślepokura Katarzyna, Lis Tadeusz, Joo Sang Woo