Repozytorium

Two-fold modification of the phenyl substituent in phenylphosphonic acid monoester monoamides.

Autorzy

Marek Stankevič

Jolanta Bazan

Rok wydania

2012

Czasopismo

Journal of Organic Chemistry

Numer woluminu

77

Strony

8244-8256

DOI

10.1021/jo301526k

Kolekcja

Naukowa

Język

Angielski

Typ publikacji

Artykuł

Streszczenie

Phenylphosphonic acid ethyl ester N,N-diethylamide was subjected to a double modification of its phenyl substituent through directed ortho-metalation followed by dearomatization of the aryl substituent under Birch reduction conditions. Application of the same methodology to a diastereomerically pure phenylphosphonic acid monoester monoamide led to the formation of P-stereogenic cyclohexadienyl-phosphonic acid derivatives. The method offers a simple and efficient modification of phenyl substituent in organophosphorus compounds.

Adres publiczny

http://dx.doi.org/10.1021/jo301526k

Strona internetowa wydawcy

https://www.acs.org/content/acs/en.html