Repozytorium

Dielectric dispersion, dilatometric and infrared studies of tris(guanidinium) enneachlorodiantimonate(III) ([C(HN2)3]3Sb2Cl9).

Autorzy

J. Zaleski

Ryszard Jakubas

Grażyna Bator

Jan Baran

Rok wydania

1994

Czasopismo

Journal of Molecular Structure

Numer woluminu

325

Strony

95-103

DOI

10.1016/0022-2860(94)80023-5

Kolekcja

Naukowa

Język

Angielski

Typ publikacji

Artykuł

Streszczenie

The results of dielectric dispersion, dilatometric and infrared studies on a new member of the family of alkylammonium halogenoantimonates ([C(NH2)3]3Sb2Cl9) are presented. A dielectric dispersion was found in a broad temperature range from 150 to 100 K. The temperature characteristic of the electric permittivity, ϵ′, measured at a static frequency (1 kHz) suggests the presence of a phase transition at about 105 K. The dilatometric studies revealed only subtle changes in the expansion coefficient at this temperature. The infrared spectra in the temperature range 14–300 K do not show any distinctive changes. The results suggest that the guanidinium cations are stabilized in a crystal lattice by weak hydrogen bonds.

Adres publiczny

https://doi.org/10.1016/0022-2860(94)80023-5

Strona internetowa wydawcy

http://www.elsevier.com

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