Repozytorium

Synthesis, spectroscopic characterization, X-ray structure and magnetic properties of [Cu(hmquin-7-COOH)2(MeOH)] complex.

Autorzy

Barbara Machura

Anna Świtlicka

Jerzy Mroziński

Julia Kłak

Rafał Kruszyński

Joachim Kusz

D. Tabak

Rok wydania

2009

Czasopismo

Polyhedron

Numer woluminu

28

Strony

3774-3780

DOI

10.1016/j.poly.2009.07.057

Kolekcja

Naukowa

Język

Angielski

Typ publikacji

Artykuł

Streszczenie

The reaction of copper(II) chloride dihydrate and 8-hydroxy-2-methylquinoline-7-carboxylic acid (Hhmquin-7-COOH) leads to [Cu(hmquin-7-COOH)2(MeOH)]. The compound has been studied by IR, UV–Vis, EPR spectroscopy and X-ray crystallography. X-ray studies confirm bidentate coordination mode of the hmquin-7-COOH anions via the pyridine nitrogen atom and deprotonated hydroxyl group. The COOH groups of the hmquin-7-COOH ligands are potentially available for further conjugation. The title complex has been additionally studied by magnetic measurement. The TDDFT/PCM calculations have been employed to discuss the electronic spectrum of [Cu(hmquin-7-COOH)2(MeOH)] in more detail.

Słowa kluczowe

Copper(II), 8-Hydroxy-2-methylquinoline-7-carboxylic acid, X-ray structure, Magnetic properties and TDDFT calculations

Adres publiczny

https://doi.org/10.1016/j.poly.2009.07.057

Strona internetowa wydawcy

http://www.elsevier.com

Podobne publikacje
2018

Copper(II) complexes of 7-amino-2-methylchromone and 7-aminoflavone: magneto-structural, spectroscopic and DFT characterization.

Mucha Paulina, Małecka Magdalena, Kupcewicz Bogumiła, Lux Karin, Dołęga Anna, Jezierska Julia, Budzisz Elżbieta